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Beilstein J. Org. Chem. 2014, 10, 1151–1158, doi:10.3762/bjoc.10.115
Graphical Abstract
Figure 1: Morpholinoglycine oligomers (A) and protected monomers 1a–e (B) for their synthesis.
Figure 2: Dangling residues of MorGly oligomers synthesized by solid phase supported (A) and liquid phase syn...
Figure 3: Cleavage of MorGly oligonucleotide mimics from solid support and deprotection of nucleobases by aqu...
Scheme 1: Synthesis of Boc-protected 2-aminomethylmorpholino nucleosides: i) di-tert-butyl dicarbonate ((Boc)2...
Scheme 2: Loading of the Boc-Gly-PAM resin with the morpholino nucleosides 5a,d,e: i) Dimethyl oxalate, TEA, ...
Figure 4: MorGly homopentamers containing adenine, uracil, and thymine nucleobases.
Beilstein J. Org. Chem. 2013, 9, 2898–2909, doi:10.3762/bjoc.9.326
Figure 1: Model compounds for the TR NMR photo-CIDNP experiments: conjugates of 4-benzoylbenzoic acid, 2’-deo...
Scheme 1: Synthesis of functionalized derivatives of 4-benzoylbenzoic acid (9), L-tryptophan (11, 16) and L-t...
Scheme 2: Synthesis of conjugates 1–3: i) 2,4,6-triisopropylbenzenesulfonyl chloride (TPSCl), 1-methylimidazo...
Scheme 3: Synthesis of conjugates 4 and 5: i) TPSCl, MeIm, Py; ii) AcOH/H2O; iii) p-chlorophenyl dichlorophos...
Scheme 4: Synthesis of conjugates 6–8. i) TPSCl, MeIm, Py; ii) TBAF in Py/H2O, then NH3/H2O; iii) TBAF in Py/H...
Beilstein J. Org. Chem. 2011, 7, 1135–1140, doi:10.3762/bjoc.7.131
Figure 1: Novel artificial RNases based on amino acids.
Scheme 1: Multicomponent approach to target molecules.
Scheme 2: Synthesis of starting diisocyanides 3a–3e.
Scheme 3: Synthesis of new aRNAses. Conditions: a. RCHO (3 eqiuv), BnNH2 (3 equiv), PhP(OH)2 (1 equiv), r.t.;...
Figure 2: Results of RT-qPCR of the TBEV RNA cleavage products in presence of 2.5 mM peptidomimetics 5a–g at ...
Figure 3: Results of RT-qPCR of the TBEV RNA cleavage products in the presence of 2.5 mM peptidomimetics afte...
Figure 4: Results of electrophoresis in 2% TBE-agarose gel with ethidium bromide of RT-qPCR products from Figure 3. (...